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Organotin based hybrid materials as selective catalysts. Hybrid organic-inorganic materials offer potential applications in a variety of fields ranging from photonics to selective catalysts. This pilot project brings together the expertise in four international research laboratories to focus on elaboration of new nanocomposites as highly selective Lewis acid catalysts for fine chemicals synthesis.
Organotin Oxo-clusters Based Hybrid Materials. Hybrid materials are composites which contain both organic and inorganic components, intimately mixed at the microscopic (nanometer) scale. They have applications in areas ranging from recoverable chemical catalysts to micro-chip technology. We will provide new oganometallic components of suitable architecture for assessment as new materials.
Mechanistic Studies on Biologically Active Iron Chelators. The need for orally effective drugs as alternatives to invasive treatment regimens such as subcutaneous infusion is an ongoing concern in health care. This is particularly true in people suffering iron overload. In many cases this condition is present at birth and thus the administration of vital iron chelation therapy via the oral route is a much preferred option. We have unearthed a novel series of candidates for iron chelation therapy ....Mechanistic Studies on Biologically Active Iron Chelators. The need for orally effective drugs as alternatives to invasive treatment regimens such as subcutaneous infusion is an ongoing concern in health care. This is particularly true in people suffering iron overload. In many cases this condition is present at birth and thus the administration of vital iron chelation therapy via the oral route is a much preferred option. We have unearthed a novel series of candidates for iron chelation therapy (the pyridine-2-carboxaldehyde isonicotinoyl hydrazone [PCIH] analogues) which show oral activity. These chelators undergo some interesting iron catalysed oxidation chemistry and it is vital that the mechanism of this reaction be elucidated to determine whether it will be of biological significance upon administration of these compounds as iron chelators.Read moreRead less
New Synthetic Routes to the Immobilisation of Mixed Valence Transition Metal Complexes on Conducting Metal Oxides. Highly coloured, electrochemically active transition metal dyes may find application electrochromic devices, where they may switch between contrasting coloured forms through a simple redox reaction. A prerequisite is that the dye be immobilised onto a solid conducting support whilst preserving the electrochemical and optical properties of the dye found in solution. This project tack ....New Synthetic Routes to the Immobilisation of Mixed Valence Transition Metal Complexes on Conducting Metal Oxides. Highly coloured, electrochemically active transition metal dyes may find application electrochromic devices, where they may switch between contrasting coloured forms through a simple redox reaction. A prerequisite is that the dye be immobilised onto a solid conducting support whilst preserving the electrochemical and optical properties of the dye found in solution. This project tackles this problem through a combination of organic and inorganic synthesis to develop new electrochromic dyes that may be attached to mesoporous titania.Read moreRead less
Ditopic receptors for the cooperative binding of cations and anions. This project is concerned with the design, synthesis and investigation of new receptor molecules that are capable of simultaneously binding metal cations and anions in a cooperative fashion. The new systems are based on a macrocyclic platform which acts as the metal binding site together with side-arms incorporating functional groups that are designed to cooperatively interact with a suitable anion. Potential applications exist ....Ditopic receptors for the cooperative binding of cations and anions. This project is concerned with the design, synthesis and investigation of new receptor molecules that are capable of simultaneously binding metal cations and anions in a cooperative fashion. The new systems are based on a macrocyclic platform which acts as the metal binding site together with side-arms incorporating functional groups that are designed to cooperatively interact with a suitable anion. Potential applications exist for this category of ditopic receptors in mineral processing where the ability to extract a metal as its metal salt may lead to more efficient solvent extraction processes.Read moreRead less
Cooperativity in Spin Crossover Systems: Memory, Magnetism and Microporosity. Spin-crossover centres are a well known form of inorganic electronic switch for which variation of temperature, pressure and irradiation leads to a change in d-electron configuration and therefore changes to structure, colour and magnetism. Here we aim to synthesise and study a wide variety of new spin-crossover systems where cooperativitiy between centres, induced by careful supramolecular design, will lead to molecul ....Cooperativity in Spin Crossover Systems: Memory, Magnetism and Microporosity. Spin-crossover centres are a well known form of inorganic electronic switch for which variation of temperature, pressure and irradiation leads to a change in d-electron configuration and therefore changes to structure, colour and magnetism. Here we aim to synthesise and study a wide variety of new spin-crossover systems where cooperativitiy between centres, induced by careful supramolecular design, will lead to molecules and materials having memory retention, magnetic ordering and/or microporosity. The significance of these aims covers several fundamental questions in the science of electronic systems. We also identify a number of potential nanochemical switching applications for the unique systems proposed.Read moreRead less
Polynuclear Spin-Crossover Molecular Switches: Host-Guest Chemistry, Magnetism and Memory. The generation of advanced nanomaterials requires both a control of nanoscale structure and the incorporation of specific properties into that structure. This project will lead to significant new developments in this area, with the assembly of complex molecular systems containing electronic switches. The unique combination of nanoscale switching and guest-binding and/or magnetic ordering in these systems ....Polynuclear Spin-Crossover Molecular Switches: Host-Guest Chemistry, Magnetism and Memory. The generation of advanced nanomaterials requires both a control of nanoscale structure and the incorporation of specific properties into that structure. This project will lead to significant new developments in this area, with the assembly of complex molecular systems containing electronic switches. The unique combination of nanoscale switching and guest-binding and/or magnetic ordering in these systems will lead to entirely new materials properties, leading in turn to fundamental advances in the science of molecular electronics and nanomaterials. Benefits of the research are wide-ranging, and include the development of innovative new technologies for molecular sensing, molecular separations, data storage and visual displays.Read moreRead less
In-situ solubility and speciation studies in super-critical H2O-NaCl-CO2 mixtures using synchrotron radiation. Understanding the physics and chemistry of metals in hypersaline and supercritical solutions represents a major scientific challenge with wide-ranging applications in the fields of mineral processing, economic geology, or CO2 sequestration. The advent of very bright sources of x-rays (synchrotrons) and development of spectroscopic cells that can contain corrosives samples at high pressu ....In-situ solubility and speciation studies in super-critical H2O-NaCl-CO2 mixtures using synchrotron radiation. Understanding the physics and chemistry of metals in hypersaline and supercritical solutions represents a major scientific challenge with wide-ranging applications in the fields of mineral processing, economic geology, or CO2 sequestration. The advent of very bright sources of x-rays (synchrotrons) and development of spectroscopic cells that can contain corrosives samples at high pressure and temperature allow for the first time the in-situ observation of these solutions. This project creates strong link between Australian and French scientists. By sharing the know-how developed at the European Synchrotron Research Facility, we aim to create a world-class facility at the Australian Synchrotron that will open in Melbourne in 2007.Read moreRead less
ENHANCED PERFORMANCE OF AUTOMOTIVE SHEET ALLOYS VIA CONTROL OF COMPOSITION, THERMAL PROCESSING AND NANOSTRUCTURE. This project involves characterisation using modern facilities of the form and identity of atomic-scale clusters of alloying elements in selected automotive sheet alloys that have been subjected to single and multiple ageing treatments and examination and modelling of deformation mechanisms and behaviour in such alloys. The aim is to establish the precise role of clusters of solute a ....ENHANCED PERFORMANCE OF AUTOMOTIVE SHEET ALLOYS VIA CONTROL OF COMPOSITION, THERMAL PROCESSING AND NANOSTRUCTURE. This project involves characterisation using modern facilities of the form and identity of atomic-scale clusters of alloying elements in selected automotive sheet alloys that have been subjected to single and multiple ageing treatments and examination and modelling of deformation mechanisms and behaviour in such alloys. The aim is to establish the precise role of clusters of solute atoms and vacancies in the formation of precipitate phases that control the final strength and deformation behaviour of the alloys, and to provide useful guidelines for further improvements in strength of these alloys via the control of alloy composition and of multiple ageing treatments.Read moreRead less
Lie-type methods for totally disconnected groups. Groups are algebraic objects which convey symmetry, much as numbers convey size. For example, the rotations of a sphere form a group. This rotation group is one of a class known as the Lie groups that is well understood and has important applications. Totally disconnected groups arise as symmetries of network structures having nodes and a `neighbour' relation between nodes. The Australian investigator has discovered powerful methods for analysing ....Lie-type methods for totally disconnected groups. Groups are algebraic objects which convey symmetry, much as numbers convey size. For example, the rotations of a sphere form a group. This rotation group is one of a class known as the Lie groups that is well understood and has important applications. Totally disconnected groups arise as symmetries of network structures having nodes and a `neighbour' relation between nodes. The Australian investigator has discovered powerful methods for analysing totally disconnected groups which have parallels with Lie group techniques. This project will develop these parallels and establish links with international researchers on Lie groups.Read moreRead less