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New Synthetic Routes to the Immobilisation of Mixed Valence Transition Metal Complexes on Conducting Metal Oxides. Highly coloured, electrochemically active transition metal dyes may find application electrochromic devices, where they may switch between contrasting coloured forms through a simple redox reaction. A prerequisite is that the dye be immobilised onto a solid conducting support whilst preserving the electrochemical and optical properties of the dye found in solution. This project tack ....New Synthetic Routes to the Immobilisation of Mixed Valence Transition Metal Complexes on Conducting Metal Oxides. Highly coloured, electrochemically active transition metal dyes may find application electrochromic devices, where they may switch between contrasting coloured forms through a simple redox reaction. A prerequisite is that the dye be immobilised onto a solid conducting support whilst preserving the electrochemical and optical properties of the dye found in solution. This project tackles this problem through a combination of organic and inorganic synthesis to develop new electrochromic dyes that may be attached to mesoporous titania.Read moreRead less
New Methods to Harvest Light: Towards Better Dye-Sensitized Solar Cells. Dye-sensitized solar cell (DSC) technology has emerged as a complementary energy source to silicon photovoltaic technology. The efficiency of the DSC relies heavily on sensitizing molecules to absorb solar photons and then transfer electrons to a semi-conducting particle. This project will investigate new sensitizing methods using a combination of different dyes which work cooperatively to absorb a large part of the solar ....New Methods to Harvest Light: Towards Better Dye-Sensitized Solar Cells. Dye-sensitized solar cell (DSC) technology has emerged as a complementary energy source to silicon photovoltaic technology. The efficiency of the DSC relies heavily on sensitizing molecules to absorb solar photons and then transfer electrons to a semi-conducting particle. This project will investigate new sensitizing methods using a combination of different dyes which work cooperatively to absorb a large part of the solar spectrum and efficiently inject electrons into a semi-conducting particles. The development and understanding of these new methods to sensitize the dye-sensitized solar cell should lead to new and better solar cells.Read moreRead less
The fate of copper in atom transfer radical reactions. Copper (Cu) complexes of poly-amine ligands have emerged as extremely active homogeneous catalysts in atom transfer radical reactions, forming organic radicals from alkyl halide precursors, and they are now employed extensively in polymer and organic chemistry. The catalyst cycles between its Cu(I) and Cu(II) oxidation states reversibly yet both forms are susceptible to side reactions, particularly with solvents which can lead to loss of cat ....The fate of copper in atom transfer radical reactions. Copper (Cu) complexes of poly-amine ligands have emerged as extremely active homogeneous catalysts in atom transfer radical reactions, forming organic radicals from alkyl halide precursors, and they are now employed extensively in polymer and organic chemistry. The catalyst cycles between its Cu(I) and Cu(II) oxidation states reversibly yet both forms are susceptible to side reactions, particularly with solvents which can lead to loss of catalytic activity. This project aims to apply a multifaceted approach to interrogate the catalysts in both their Cu(I) and Cu(II) oxidation states and identify for the first time the pathways that lead to undesirable side reactions and provide new ways of optimising catalyst performance.Read moreRead less
Advanced Molecular Frameworks for Sodium Battery Electrode Applications. This project aims to develop new molecular materials capable of high capacity sodium-ion insertion. Through an innovative interdisciplinary approach that targets the synthesis and detailed characterisation of an extensive family of materials this project expects to generate major advances in the understanding of how the chemical, physical and structural attributes of the materials relate to their electrical charge/discharge ....Advanced Molecular Frameworks for Sodium Battery Electrode Applications. This project aims to develop new molecular materials capable of high capacity sodium-ion insertion. Through an innovative interdisciplinary approach that targets the synthesis and detailed characterisation of an extensive family of materials this project expects to generate major advances in the understanding of how the chemical, physical and structural attributes of the materials relate to their electrical charge/discharge behaviours. Significant anticipated outcomes and benefits include the development of new material design approaches that optimise battery electrode performance across a diverse parameter space, and the generation of advanced new materials worthy of commercial development in low-cost, large-scale battery applications.Read moreRead less
Polyoxometalate Clusters: Catalytic Chemistry in Solution and Condensed States. Polyoxometalate cluster anions are soluble metal-oxygen clusters that are cheap, robust and non-toxic.
Conditions for systematic tuning of redox potentials over the range +2 to -3 V have become accessible via certain photo-active polyoxometalates. The same system can provide powerful oxidants (that rival chlorine) and powerful reductants (that rival potassium).
The program will take advantage of this unique ....Polyoxometalate Clusters: Catalytic Chemistry in Solution and Condensed States. Polyoxometalate cluster anions are soluble metal-oxygen clusters that are cheap, robust and non-toxic.
Conditions for systematic tuning of redox potentials over the range +2 to -3 V have become accessible via certain photo-active polyoxometalates. The same system can provide powerful oxidants (that rival chlorine) and powerful reductants (that rival potassium).
The program will take advantage of this unique range of properties to explore:-
(i) coupling of photo- and electro-chemical processes into effective catalytic cycles;
(ii) photo- and electro-chemical processes in ionic liquid solvents;
(iii) synthesis and redox reactivity of nanoparticles stabilised by polyoxometalates.
Read moreRead less
Short circuiting redox enzymes. Enzymes that catalyse oxidation or reduction reactions can be integrated with an electrode in the development of biosensors. A key challenge is enabling an electrical current between the enzyme and the electrode and this project aims to probe this phenomenon to provide an enzyme system that operates with greater efficiency than in nature.
Linkage Infrastructure, Equipment And Facilities - Grant ID: LE180100168
Funder
Australian Research Council
Funding Amount
$264,706.00
Summary
A glow discharge optical emission spectrometer for challenging surfaces. This project aims to address a critical surface characterisation gap in Australian research by the implementation of a glow-discharge optical emission spectrometer. Determining the composition depth profile of chemically complex surfaces that are rough, fragile, and air-sensitive is very challenging. The project will allow rapid and accurate elemental depth profiling of surface layers up to hundreds of microns in thickness ....A glow discharge optical emission spectrometer for challenging surfaces. This project aims to address a critical surface characterisation gap in Australian research by the implementation of a glow-discharge optical emission spectrometer. Determining the composition depth profile of chemically complex surfaces that are rough, fragile, and air-sensitive is very challenging. The project will allow rapid and accurate elemental depth profiling of surface layers up to hundreds of microns in thickness and with nanometre resolution. Critically this instrument allows glovebox-to-instrument analysis without surface preparation, preserving the in-situ state of the surface. This will fast-track research in battery materials, new methods to control corrosion, and the design of advanced engineered surfaces.Read moreRead less
Pioneering stable copper carbanions for new C-C bond forming paradigms. The stabilisation of highly reactive carbanions underpins advances in chemical synthesis of new compounds including polymers, agrichemicals and pharmaceuticals. This project aims to deliver an innovative chemical reactivity platform, underpinned by copper carbanion complexes accessed via synthetic electrochemistry. Carbanions are essential components of carbon-carbon bond forming reactions but their high reactivity can be pr ....Pioneering stable copper carbanions for new C-C bond forming paradigms. The stabilisation of highly reactive carbanions underpins advances in chemical synthesis of new compounds including polymers, agrichemicals and pharmaceuticals. This project aims to deliver an innovative chemical reactivity platform, underpinned by copper carbanion complexes accessed via synthetic electrochemistry. Carbanions are essential components of carbon-carbon bond forming reactions but their high reactivity can be problematic. Expected outcomes of this project are an understanding of why these novel copper compounds are stable and how they can be utilised as synthetic reagents. This should provide significant benefits in unlocking the synthetic potential of a new class of chemical compound that has until now remained unexplored.Read moreRead less
Titanium Electrochemistry in Minerals Processing. Australia is on of the world's largest producers of titanium minerals for industrial and consumer products. This project aims to improve the efficiency of the Sulfate Process which is used to convert the titanium containing ore ilmenite into pure titanium dioxide pigment. The impovements expected include a decrease in the cost of production for the relevant industries, as well as a reduction in the volume of waste materials generated by the proce ....Titanium Electrochemistry in Minerals Processing. Australia is on of the world's largest producers of titanium minerals for industrial and consumer products. This project aims to improve the efficiency of the Sulfate Process which is used to convert the titanium containing ore ilmenite into pure titanium dioxide pigment. The impovements expected include a decrease in the cost of production for the relevant industries, as well as a reduction in the volume of waste materials generated by the process. Read moreRead less
Electrochemically-sensitized luminescence: A new bio-detection paradigm. This project aims to create new science which will enable the development of a superior new class of bio-detection technique, suitable for medical diagnostics and other sensing applications. A multi-disciplinary approach will be taken, combining expertise in a number of fields to explore the use of electrical rather than traditional optical means to control energy transfer and luminescence in novel molecular and nanoparticl ....Electrochemically-sensitized luminescence: A new bio-detection paradigm. This project aims to create new science which will enable the development of a superior new class of bio-detection technique, suitable for medical diagnostics and other sensing applications. A multi-disciplinary approach will be taken, combining expertise in a number of fields to explore the use of electrical rather than traditional optical means to control energy transfer and luminescence in novel molecular and nanoparticle-based systems. It is expected that these advances will transform bio-analytical science by giving rise to innovative detection techniques which are low-cost, rapid and highly sensitive.Read moreRead less